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Anion Analysis Lab

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Introduction
Identification of ionic compounds is imperative for food, medicine and drug scientists to understand. If ionic compounds present in items such as food and drugs cannot be properly identified, the foodstuff and drug items put the consumer at risk of putting something into their bodies that could potentially cause them harm. During this project we used a variety of elimination and confirmation tests to test 4 known cations and 4 known anions in order to construct logic trees. The logic trees for both the cation and anion tests that we developed in parts 1 and 2 of this project were used to determine the identity of an unknown ionic compound in part 3. The objective of both the anion and cation elimination and confirmation tests …show more content…
Cation Analysis
Approximately 0.5 grams of the unknown ionic solid was gathered and was dissolved with 5 mL of distilled water in a clean, dry centrifuge tube. The solution dissolved in water and became our stock solution for testing. All the steps from Part 1 of this experiment were then repeated on our stock solution to analyze the cation in the unknown solid.
Anion Analysis
Approximately 0.1 grams of our unknown ionic solid and 0.5 grams of anhydrous sodium carbonate were weighed out and placed in a 50 mL beaker with 5mL of water and a boiling chip prior to heating the mixture. A pencil was used to mark a line on the beaker to show the initial level for the solvent. The solution was then heated for 10 minutes on a hot plate, making sure to maintain a 5mL level of solvent with the addition of distilled water. The mixture was then transferred equally into two centrifuge tubes and was centrifuged to isolate any left over precipitate and remove it from the solution entirely. The liquid solution that we were left with after removing the precipitate was the stock solution we used for testing. All the steps from Part 2 of this experiment were then repeated on our stock solution to analyze the anion in the unknown

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