...“The Project” An Unknown Ionic Compound in the Landfill Introduction Upon discovery of an unknown solid ionic compound in a landfill by the Chemistry 1146 laboratory group, precautions were immediately taken and rigorous experimentations were begun to determine the identity of the compound. Determining the identity of this compound was very crucial for the safety of the community. The chemical and physical properties of the compound could then be identified and environmental hazards addressed. Questions that needed to be answered in relation to this unknown compound included: Is it a risk to people living nearby? What if it gets in the water supply? Does it contaminate the air? Is it reactive? Over a three week time-span the chemists experimented with the unknown compound to report the findings back to the community. After the unknown compound was identified, the chemists studied its properties and confirmed the identity by synthesizing the compound in the lab and comparing it to the unknown. Experimental Week 1 After a sample of the unknown compound (#21) was retrieved, various experiments were carried out to determine the chemical formula. An anion analysis was first performed on the unknown compound. A solution of the unknown compound was prepared by taking a small amount of the solid on the end of a scoopula and dissolving it in 2 mL of distilled water (DI water) in a test tube. The compound was then tested for the sulfate ion by placing 1 mL of the solution in a test...
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...can use stoichiometry to calculate masses, moles, and percents within a chemical equation. ________________________________________ ________________________________________ What is a Chemical Equation? In chemistry, we use symbols to represent the various chemicals. Success in chemistry depends upon developing a strong familiarity with these basic symbols. For example, the symbol "C"represents an atom of carbon, and "H" represents an atom of hydrogen. To represent a molecule of table salt, sodium chloride, we would use the notation "NaCl", where "Na" represents sodium and "Cl" represents chlorine. We call chlorine "chloride" in this case because of its connection to sodium. You should have reviewed naming schemes, or nomenclature, in earlier readings. A chemical equation is an expression of a chemical process. For example: AgNO3(aq) + NaCl(aq) ---> AgCl(s) + NaNO3(aq) In this equation, AgNO3 is mixed with NaCl. The equation shows that the reactants (AgNO3 and NaCl) react through some process (--->) to form the products (AgCl and NaNO3). Since they undergo a chemical process, they are changed fundamentally. Often chemical equations are written showing the state that each substance is in. The (s) sign means that the compound is a solid. The (l) sign means the substance is a liquid. The (aq) sign stands for aqueous in water and means the compound is dissolved in water. Finally, the (g) sign means that the compound is a gas. Coefficients are used in all chemical equations...
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...CH 220C ORGANIC CHEMISTRY LABORATORY Spring, 2015 Section Page 1. General Information 2 2. Safety Information 2 3. Attendance 3 Make-Up Policy 3 4. Laboratory Protocol 3 Assigned Reading 3 Pre-Lab Quizzes 3 Lab Notebook 5 Chemicals 5 Due Dates for Reports 5 5. Orientation 5 In-Lab Information 5 Library Information 5 6. Check-In 6 7. Grading Procedure 6 8. Policy on Cheating 7 9. TA Office Hours 8 10. Faculty Course CoordinatorS 8 11. Course Web Page 8 12. Hints to Minimize Frustration IN ORGANIC CHEMISTRY 8 13. Work Schedule 10 Lab Report Due Date Schedule 10 Experiments 10 14. Supplements 17 A. Extraction of Unknown 17 B. Recrystallization of Unknown Products 18 C. Methyl Benzoate 19 D. Synthesis of Luminol 20 E. Azo Violet 23 1. GENERAL INFORMATION PRE- and CO-REQUISITES Pre- and co-requisites for CH 220C listed in the Course Schedule. Important: Because the lecture and laboratory courses are co-requisites of each other, dropping one of them requires that you drop the other as well, unless the drop occurs during ...
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...The Determination of Boiling Points and Melting Points of Organic Compounds During this laboratory session, we will practice determining the boiling point of a liquid organic compound and the melting point (or we could call it the freezing point) of a solid organic compound. The boiling point of a liquid is the temperature at which the pressure of the vapor above a liquid equals the existing pressure. As we heat a liquid, the pressure of the vapor above the liquid slowly increases. When this pressure equals the pressure existing in the container, the liquid begins to boil– the liquid turns to vapor. If not contained, the vapor will “escape” into the atmosphere. In other words, the liquid evaporates. If the vapor is contained, and then passed through an area where the temperature is lower, the vapor will “condense” and enter the liquid state again. This would be a distillation. Atmospheric pressure is approximately 760 mm Hg; i.e., the weight of a column of mercury measuring 1 mm2 and 760 mm tall. This equates to about 29.7 inches of mercury. If we reduce the pressure above the sample that we are heating, we can reduce the boiling point of the liquid. This is referred to as a vacuum distillation or carrying out a distillation in vacuo. For example, while water boils at 100oC (or 212° F) at 760 mm Hg, it boils around 22oC at 20 mm Hg. The boiling point of a liquid is a physical characteristic of a compound. Many factors go into the estimation of the boiling point of a liquid such...
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...The Determination of Boiling Points and Melting Points of Organic Compounds During this laboratory session, we will practice determining the boiling point of a liquid organic compound and the melting point (or we could call it the freezing point) of a solid organic compound. The boiling point of a liquid is the temperature at which the pressure of the vapor above a liquid equals the existing pressure. As we heat a liquid, the pressure of the vapor above the liquid slowly increases. When this pressure equals the pressure existing in the container, the liquid begins to boil– the liquid turns to vapor. If not contained, the vapor will “escape” into the atmosphere. In other words, the liquid evaporates. If the vapor is contained, and then passed through an area where the temperature is lower, the vapor will “condense” and enter the liquid state again. This would be a distillation. Atmospheric pressure is approximately 760 mm Hg; i.e., the weight of a column of mercury measuring 1 mm2 and 760 mm tall. This equates to about 29.7 inches of mercury. If we reduce the pressure above the sample that we are heating, we can reduce the boiling point of the liquid. This is referred to as a vacuum distillation or carrying out a distillation in vacuo. For example, while water boils at 100oC (or 212° F) at 760 mm Hg, it boils around 22oC at 20 mm Hg. The boiling point of a liquid is a physical characteristic of a compound. Many factors go into the estimation of the boiling point of a liquid such...
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...Lab Report Chemistry 341L: Preparation of Cyclohexene Introduction: The purpose of this lab was to prepare an alkene, cyclohexene, by the dehydration of an alcohol, cyclohexanol. In this experiment cyclohexanol is dehydrated to prepare cyclohexene, using phosphoric acid as a catalyst. Unsaturation tests are then done to ensure cyclohexene was prepared. Experimental Scheme: The procedure for the Preparation of Cyclohexene lab started with first having to add 10mL of cylcohexanol (clear liquid with strong odor), and 2.5mL of phosphoric acid (clear liquid) to a 50-mL round bottom flask. These liquids were mixed together well; a boiling stone was added to the flask in order to allow for a smoother and gentle boil. Below is the equation for the reaction that took place in this lab. Equation 1: Formation of the product cyclohexene, from the reactant cyclohexanol with the aid of a catalyst phosphoric acid4 Next a distillation apparatus had to be assembled, using a 25-mL round bottom flask as a receiving flask, this flask was then placed into a beaker of ice water refer to figure 1. Figure 1: Distillation apparatus5 Distillation is used in order to dehydrate the cyclohexanol. After the apparatus was assembled we circulated the cooling water in the condenser, while heating the mixture in the flask. The flask was heated until the product started to distill, and collect into the receiving flask in the ice water bath. We continued to heat the mixture...
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...Lab Report Marco Huerta Partner: Sami Mrestani Chem 12B – Organic Chemistry 11/07/11 Lazik Benzocaine Objective: To prepare a local anesthetic, Benzocaine, by the direct estherification of p-aminobenzoic acid with ethanol. Abstract: Over the years many new local anesthetics have been synthesized and tested. Though many have not come into general use, the search for the perfect local anesthetic is still under way. An interesting fact about these compounds is that they all share common feature (see general structure below). At one end of the molecule is an aromatic ring. At the other is a secondary or tertiary amine. These two ends are separated by a central chain of atoms usually one to four units long. The aromatic part is typically and ester of an aromatic acid which is important to the bodily detoxification of these compounds. In our experiment, we created a topical anesthetic, Benzocaine, by the direct estherification of p-aminobenzoic acid. This was accomplished by reaction with absolute ethanol catalyzed by concentrated sulfuric acid and later neutralized with a 10% sodium carbonate solution. Neutralization raised the pH of the overall reaction system to about 8 creating a precipitate of Benzocaine. Recrystallization of the crude product was performed to increase purity. Our...
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...Volumetric and Vinegar Analysis Abstract This report presents volumetric and vinegar analysis. In volumetric analysis three trials of a solution. The volumetric analysis was obtained through titration, and chemical analysis, which allowed the molar concentration of a strong acid to be assessed in a standardized solution. The Average molar concentration of NaOH is approximately 0.279mol/L. Vinegar analysis was conducted with the help of three trials to determine the percent by mass of acetic acid in vinegar instead of a standardized solution. The unknown vinegar being utilized was “Shaggy”. The average percent by mass of CH3COOH “Shaggy” is 1.41%. According to “Laboratory Manual for Principles of General Chemistry”, volumetric analysis is a chemical analysis that is performed primarily with the aid of volumetric glassware. For this procedure, a known quantity or carefully measured amount of one substance reacts with a to-be-determined amount of another substance with the reaction occurring in an aqueous solution. This is conducted by a titration procedure. A burette dispenses a liquid called the titrant to a receiving flask containing the analyte (Beran, 133). The reaction is known to be completed when amounts corresponding to the mole ratio of the balanced equation is reached – this is referred to as the stoichiometric point. In the lab, standardization of a sodium hydroxide solution was performed, thus creating the secondary standard solution (Beran, 135)...
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...CHEG 231011 Thermodynamics I Project Report Compound: Dimethyl Sulfide (C2H6S) Abstract: This project focuses on the thermodynamic properties of dimethyl sulfide (C2H6S). This report mainly consist of a basic introduction for C2H6S from chemical, physical, environmental, industrial sights, a methodology part to show how to generate the thermodynamic charts and a rankine refrigeration cycle for C2H6S, a result part of all the charts and cycle I get from mat lab and other calculation methods, a brief discussion part between the thermodynamic charts and the chemical, physical, environmental, industrial significance. Introduction 1. Basic chemistry. C2H6S: Structure: [pic] [pic] Molecular weight: 62.134 Boiling Point: 38 °C (311 °K) Freezing Point: -98.72 °C (174.88 °K) Triple Point Temperature (Ttri): 174.85°K Critical Temperature (Tc): 503 °K Critical Pressure (Pc): 55.30 bar Critical Molar Volume (Vc): 0.2066 L/mol Critical compressibility factor (Zc):0.273 Acentric factor (ω): 0.191 Antoine Equation Parameters A: 4.28713, B: 1201.134, C: -29.906 2. Compound uses. Dimethyl sulfide (DMS) is a key compound in global sulfur and carbon cycles. a) chemical reactant Dimethyl Sulfide will undergo some types of reactions and used as a source to produce several chemical compounds. [pic] (b) Food and Beverage Component DMS is a primary aroma and flavor compound to make beer character. It is also used in other food applications...
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...[pic] Official TCC Course Syllabus |Discipline Prefix: CHM |Course Number: 111 |Course Title: College Chemistry I | | |Course Section: D04B | | |Credit Hours: 4 |Lecture Hours: 3 |Clinical Hours: |Lab Hours: 3 | |Contact Hours: 6 |Studio Hours: N/A |Semester: Fall | |Meeting Days/Time/Location: Fridays/1:30pm-4:20pm/Science Building | Instructor Information Name: Dr. Shahin Maaref Office Location: JD-30 Office Hours: TRF 9:00am-11:00am, TR 4:30pm-5:30pm & by appointment Contact Information: 822-7692 Blackboard site: http://learn.vccs.edu Instructor email address: smaaref@tcc.edu Course Information Course Description Explores the fundamental laws, theories, and mathematical concepts of chemistry. Designed primarily for science and engineering majors. Requires a strong background in mathematics. Part I of II. Prerequisites and/or Co-requisites Prequisites - None Corequisites – None It is recommended to have H.S. chemistry or CHM01 as prerequisites and MTH 03 or MTE 06 level or higher. ...
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...NUTRITION 121 HUMAN NUTRITION LABORATORY BACKGROUND AND METHODS MODULE #1 BODY COMPOSITION Late Labs: 10 point deduction! A report submitted >1 week late, will receive 0 points for the lab!! Written and edited by: Karon Felten and Nutrition 121 TA’s With Special Thanks to: Chris Pritsos Ph.D. Nutrition Department Chairman ABSTRACT: In nutrition, there are many factors that influence an individual’s health and body weight, such as heredity, food selection, eating behaviors, and physical activity. Scale weight is not always a good indicator of body fat, lean mass, body water or overall health (1). This laboratory experience will give students the opportunity to conduct physical assessments by evaluating body weight and body composition. To determine body weight and body composition, techniques such as bioelectrical impedance analysis (BIA), body mass index (BMI), waist circumference, wrist circumference for determining frame size, and a scale will be utilized. Students will also evaluate their own risk for cardiovascular disease and assess cardiovascular health in volunteers by measuring heart rate, filling out a heart disease risk score form, and estimating oxygen consumption and energy expenditure through a technique known as the Queens College Three-Minute Step Test. BACKGROUND: Your body is made up of the six essential nutrients: water, fat, protein, carbohydrates and various vitamins and minerals. Many factors can influence an individual’s...
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...oxidation-reduction reactions for determining the oxidizing capacity of bleach. Initially an excess of iodide ions are added to a bleach solution. The iodide ions are oxidized to iodine after the solution has been acidified. Starch is added to the resulting iodine solution as an indicator. The solution is then titrated with sodium thiosulfate until the color of the solution changes indicating the endpoint of the reaction. Data collected from the titrations will be used to calculate the mass of the sodium hypochlorite in an unknown solution of bleach. Given the original mass of the unknown solution and the calculated mass of the sodium hypochlorite in the unknown solution, the percent by mass of the sodium hypochlorite can be determined. The oxidizing capacity of the unknown bleach is effectively the percent by mass of the sodium hypochlorite in the unknown bleach sample. OJECTIVES 1) Titration of a sample of bleach with thiosulfate. 2) Determining the end point of the titration with starch indicator. 3) To determine oxidizing capacity of bleach by determining the percentage by mass of the bleach that is sodium hypochlorite. 4) Balance and summarize the two redox reactions to determine the overall chemical reaction that occurs during the titration. PRINCIPLES Oxidizing Capacity of Bleach The effectiveness of a bleach to whiten and remove stains in white clothing is related to the oxidizing (bleaching) strength of an oxidizing agent, such as OCl−, which is found in common...
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...http://www.labcompliance.com/tutorial/methods/default.aspx?sm=d_d TutorialHome | Contact Us | Newsletter | Usersclub | Books | Audio Seminars Seminars Audio Seminars Video Seminars Workshops Literature Books SOPs Validation Examples Free Literature Glossary Usersclub Intro Log-in Register Preview Renewal Tutorials Risk Management Practices Computer Validation Part11 Method Validation ISO 17025 Lab Equipment Qualification Good Laboratory Practices About About Labcompliance Contact Labcompliance Scope Tax/Bank Information All come with 10+ Best Practice Documents: SOPs, Checklists, Examples Transfer of Analytical Procedures According to the New USP Chapter <1224> With SOPs, templates and examples for easy implementation March 21, 2013 Quality by Design (QbD) for Analytical Method Development and Validation Learn how to design robustness for easy transfer and to avoid OOS situations Recorded, available at any time Validation of Analytical Methods for GLP and Clinical Studies Learn how to design, prepare, conduct and document for FDA compliance Recorded, available at any time Eight Steps for Cost-effective Laboratory Compliance Up-to-date overview, hot topics and trends. Recorded, available at any time Verification of Compendial Methods according to the New USP Chapter <1226> Understand the new risk based approach and and get real world case studies for testing Recorded, available...
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...Lab Manual Introductory Biology (Version 1.4) © 2013 eScience Labs, LLC All rights reserved www.esciencelabs.com • 888.375.5487 2 Table of Contents: Introduc on: Lab 1: Lab 2: Lab 3: Lab 4: The Scien fic Method Wri ng a Lab Report Data Measurement Introduc on to the Microscope Biological Processes: Lab 5: Lab 6: Lab 7: Lab 8: Lab 9: The Chemistry of Life Diffusion Osmosis Respira on Enzymes The Cell: Lab 10: Lab 11: Lab 12: Lab 13: Lab 14: Lab 15: Cell Structure & Func on Mitosis Meiosis DNA & RNA Mendelian Gene cs Popula on Gene cs 3 4 Lab Safety Always follow the instruc ons in your laboratory manual and these general rules: eScience Labs, LLC. designs every kit with safety as our top priority. Nonetheless, these are science kits and contain items which must be handled with care. Safety in the laboratory always comes first! Lab Prepara on • • Please thoroughly read the lab exercise before star ng! If you have any doubt as to what you are supposed to be doing and how to do it safely, please STOP and then: Double-check the manual instruc ons. Check www.esciencelabs.com for updates and ps. Contact us for technical support by phone at 1-888-ESL-Kits (1-888-375-5487) or by email at Help@esciencelabs.com. • Read and understand all labels on chemicals. If you have any ques ons or concerns, refer to the Material Safely Data Sheets (MSDS) available at www.esciencelabs.com. The MSDS lists the dangers, storage requirements, exposure treatment...
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...Fooling the Bladder Cops: The Complete Drug Testing Guide Justin Gombos June 1, 1999 2 Contents 1 Introduction 2 Detection Times 2.1 Halflife of TetraHydraCannabinol . . . . . . . . . . . 2.2 Approximate Detection Times of Various Substances 2.2.1 Frequency of Intake . . . . . . . . . . . . . . . 2.2.2 Amount of Body Fat . . . . . . . . . . . . . . 2.2.3 Predicting Detection Period . . . . . . . . . . 2.3 Positive (defined) . . . . . . . . . . . . . . . . . . . . 2.3.1 Passive smoke and positives . . . . . . . . . . 2.4 Decreasing detection times . . . . . . . . . . . . . . . 2.4.1 Physical Activity . . . . . . . . . . . . . . . . 2.4.2 Diet . . . . . . . . . . . . . . . . . . . . . . . 2.4.3 Using Drugs to Reduce Detection Times . . . 3 Test Methods 3.1 Substances that are Detectable . . . . . . . . . . . 3.2 DrugAlert . . . . . . . . . . . . . . . . . . . . . . . 3.3 Gas Chromatography . . . . . . . . . . . . . . . . . 3.4 Gas Chromatography / Mass Spectrometry . . . . . 3.5 Hair testing . . . . . . . . . . . . . . . . . . . . . . 3.6 High Performance Liquid Chromatography . . . . . 3.7 ImmunoAssay . . . . . . . . . . . . . . . . . . . . . 3.7.1 Radio ImmunoAssay (aka AbuScreen) . . . 3.7.2 Enzyme Multiplied Immunoassay Technique 3.7.3 Fluorescence Polarization ImmunoAssay . . 3.8 PharmChek . . . . . . . . . . . . . . . . . . . . . . 3.9 TestCup . . . . . . . . . . . . . . . . . . . . . . . . 3 11 13 13 13 15 16 16 16 17 17 18 18 18 19 19 21 21 21 22 24 24 25 25 25 26...
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