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Nt1310 Unit 4 Assignment 2

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The following provides more clarification and information you requested in your letter dated 08/24/15.

For Item 12, which concerned an average response calibration fit for DRO observed >20% RSD, attached find e-mail correspondence to Agilent Technical Support team. They confirmed a software issue that a linear fit it is not quantifying values correctly that they need to address.
They recommended using “force zero on” until they are able to provide a software update.

The following table compares 06/09/15 results from the RF, the linear curve with the “force zero off” and the linear curve with the “force zero on.”

Attached find calibration data now meets method specifications. The attached represents calibration data from 06/15/15 and shows the average RF is 14 percent, which is with the method acceptance criterion. The laboratory will continue to use the RF when it is ≤20 RSD and use the linear – “force zero on” when the RF is >20 RSD. …show more content…
Appendix A in each SOP indicates the updated changes. For SOP O-8620.10, Appendix I was added to specifiy surrogate requirements for West Virginia samples. For SOP O-8621.5, Appendix H was added to incorporate column performance requirements for West Virginia

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